Urinary collagen type II C-telopeptide fragments are sensitive markers of matrix metalloproteinase-dependent cartilage degradation in rat adjuvant-induced arthritis

J Rheumatol. 2003 Jul;30(7):1561-4.

Abstract

Objective: To assess the relevance of collagen type II C-telopeptide fragments (CTX-II) as markers of cartilage degradation during adjuvant-induced arthritis in rats.

Methods: Rats were injected with Freund's adjuvant on day 0 and treated orally for 21 days twice a day with vehicle or 10 or 20 mg/kg of a newly designed matrix metalloproteinase inhibitor (MMP-Inh). Urine samples were collected for 24 h between days 19 and 20 and the concentration of the cartilage-derived CTX-II was measured with a 2-site, sandwich-type ELISA. To assess arthritis, inflammatory scores were determined, and changes in paw volumes were measured by plethysmography.

Results: On day 21, the inflammation was generalized in rats injected with Freund's adjuvant. The urinary concentration of CTX-II was significantly higher in arthritic rats than in control non-injected rats. Oral treatment of arthritic rats with MMP-Inh dramatically decreased the concentration of CTX-II in urine, with values returning to those of controls. Treatment simultaneously reduced the clinical variables of the disease.

Conclusion: These results demonstrate that fragments of type II collagen in urine can be used as a measure of cartilage degradation in arthritic rats as well as potent non-invasive markers of the efficacy of chondroprotective treatments.

MeSH terms

  • Animals
  • Arthritis, Experimental / enzymology*
  • Arthritis, Experimental / physiopathology
  • Arthritis, Experimental / urine
  • Cartilage, Articular / drug effects
  • Cartilage, Articular / enzymology*
  • Collagen / urine
  • Collagen Type I
  • Collagen Type II / urine*
  • Enzyme Inhibitors / pharmacology
  • Female
  • Freund's Adjuvant
  • Inhibitory Concentration 50
  • Matrix Metalloproteinase Inhibitors
  • Matrix Metalloproteinases / metabolism*
  • Peptide Fragments / urine
  • Peptides / urine
  • Rabbits
  • Rats
  • Rats, Inbred Lew

Substances

  • Collagen Type I
  • Collagen Type II
  • Enzyme Inhibitors
  • Matrix Metalloproteinase Inhibitors
  • Peptide Fragments
  • Peptides
  • collagen type I trimeric cross-linked peptide
  • Collagen
  • Freund's Adjuvant
  • Matrix Metalloproteinases