Ligand screening by exoproteolysis and mass spectrometry in combination with computer modelling

J Mol Biol. 2003 Jul 25;330(5):1039-48. doi: 10.1016/s0022-2836(03)00664-8.

Abstract

Here, we present a new approach for protein ligand screening based on the use of limited exoproteolysis coupled to MALDI-TOF mass spectrometry, combined with computational modelling and prediction of binding energies. As a test for this combined approach, we have screened a combinatorial library containing 8000 peptides (organized in 60 peptide samples) based on positional scanning format. This library is attached to a poly-Pro framework, and screened against the Abl-SH3 domain. The results obtained demonstrated the validity of the experimental and theoretical approaches in identifying better ligands and in rationalizing the changes in affinity. Exoproteolysis coupled to MALDI-TOF mass spectrometry could be used to screen complex libraries in a fast and efficient way.

MeSH terms

  • Algorithms
  • Coumaric Acids / chemistry
  • Gene Library
  • Humans
  • Ligands*
  • Mass Spectrometry
  • Models, Molecular
  • Peptide Library
  • Peptides / chemistry
  • Protein Binding
  • Protein Structure, Tertiary
  • Proteins / metabolism*
  • Software
  • Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization
  • src Homology Domains

Substances

  • Coumaric Acids
  • Ligands
  • Peptide Library
  • Peptides
  • Proteins
  • sinapinic acid