Expression of EGFP-amino-tagged human mu opioid receptor in Drosophila Schneider 2 cells: a potential expression system for large-scale production of G-protein coupled receptors

Protein Expr Purif. 2003 Sep;31(1):123-32. doi: 10.1016/s1046-5928(03)00140-2.

Abstract

The G-protein coupled receptor (GPCR) human mu opioid receptor (hMOR) fused to the carboxy-terminus of the enhanced green fluorescent protein (EGFP) has been successfully and stably expressed in Drosophila Schneider 2 cells under the control of an inducible metallothionein promoter. Polyclonal cells expressing EGFPhMOR display high-affinity, saturable, and specific binding sites for the opioid antagonist diprenorphine. Competition studies with opioid agonists and antagonists defined the pharmacological profile of a mu opioid receptor similar to that observed in mammalian cells, suggesting proper folding of EGFPhMOR in a high-affinity state in Drosophila cells. The functionality of the fusion protein was demonstrated by the ability of agonist to reduce forskolin-stimulated cyclic AMP production and to induce [35S]GTPgammaS incorporation. The EGFPhMOR protein had the expected molecular weight (70kDa), as demonstrated by protein immunoblotting with anti-EGFP and anti-C-terminus hMOR antibodies. However, quantitative EGFP fluorescence intensity analysis revealed that the total level of expressed EGFPhMOR is 8-fold higher than the level of diprenorphine binding sites, indicating that part of the receptor is not in a high-affinity state. This may in part be due to a population of receptors localized in intracellular compartments, as shown by the distribution of fluorescence between the plasma membrane and the cell interior. This study shows that EGFP is a valuable and versatile tool for monitoring and quantifying expression levels as well as for optimizing and characterizing an expression system. Optimization of the Drosophila Schneider 2 cell expression system will allow large-scale purification of GPCRs, thus enabling structural studies to be undertaken.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Binding, Competitive / drug effects
  • Blotting, Western
  • Cell Line
  • Cloning, Molecular
  • Colforsin / pharmacology
  • Copper Sulfate / pharmacology
  • Cyclic AMP / metabolism
  • DNA, Complementary / genetics
  • Diprenorphine / metabolism
  • Diprenorphine / pharmacology
  • Drosophila / cytology
  • Enkephalin, Ala(2)-MePhe(4)-Gly(5)- / pharmacology
  • GTP-Binding Proteins / metabolism
  • Gene Expression / drug effects
  • Genetic Vectors / genetics
  • Green Fluorescent Proteins
  • Guanosine 5'-O-(3-Thiotriphosphate) / pharmacology
  • Humans
  • Luminescent Proteins / biosynthesis*
  • Luminescent Proteins / genetics
  • Metallothionein / genetics
  • Microscopy, Confocal
  • Morphine / pharmacology
  • Naloxone / pharmacology
  • Naltrexone / pharmacology
  • Oligopeptides / metabolism
  • Oligopeptides / pharmacology
  • Opioid Peptides
  • Pertussis Toxin / pharmacology
  • Polymerase Chain Reaction
  • Protein Binding / drug effects
  • Receptors, G-Protein-Coupled / biosynthesis
  • Receptors, G-Protein-Coupled / genetics
  • Receptors, Opioid, mu / biosynthesis*
  • Receptors, Opioid, mu / genetics
  • Receptors, Opioid, mu / physiology
  • Recombinant Fusion Proteins / biosynthesis*
  • Recombinant Fusion Proteins / metabolism
  • Spectrometry, Fluorescence
  • Thermodynamics

Substances

  • DNA, Complementary
  • Luminescent Proteins
  • Oligopeptides
  • Opioid Peptides
  • Receptors, G-Protein-Coupled
  • Receptors, Opioid, mu
  • Recombinant Fusion Proteins
  • Enkephalin, Ala(2)-MePhe(4)-Gly(5)-
  • Green Fluorescent Proteins
  • Diprenorphine
  • Colforsin
  • dermorphin
  • Naloxone
  • Guanosine 5'-O-(3-Thiotriphosphate)
  • Naltrexone
  • Morphine
  • Metallothionein
  • Cyclic AMP
  • Pertussis Toxin
  • GTP-Binding Proteins
  • Copper Sulfate