Adeno-associated virus Rep78/Rep68 promotes localized melting of the rep binding element in the absence of adenosine triphosphate

Chembiochem. 2004 Mar 5;5(3):324-32. doi: 10.1002/cbic.200300737.

Abstract

We have applied fluorescence anisotropy and molecular beacon fluorescence methods to study the interactions between the Adeno-associated virus Rep78/Rep68 protein and the 23-bp Rep binding element (RBE). Rep78/Rep68 stably interacted with both the single- and double-stranded conformations of the RBE, but the interaction mechanisms of single- and double-stranded DNA appeared to be fundamentally different. The stoichiometry of Rep78 association with both the separate top and bottom strands of the RBE was 1:1, and the relative dissociation constant (K(D)) values of these associations were calculated to be 2.3x10(-8) and 3.2x10(-8) M, respectively. In contrast, the stoichiometry of Rep78 association with the double-stranded RBE was 2:1, and the dissociation constant was determined to be 4.2x10(-15) M(2). Moreover, Rep78/Rep68 interaction with the 23-bp duplex RBE appeared to cause localized melting of the double-stranded DNA substrate in the absence of adenosine triphosphate (ATP). This melting activity showed slower kinetics than binding and may contribute to the initiation of ATP-dependent Rep78 helicase activity.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Adenosine Triphosphate*
  • Adenoviridae / chemistry
  • Adenoviridae / genetics
  • DNA Helicases
  • DNA, Single-Stranded / metabolism
  • DNA, Viral / chemistry
  • DNA, Viral / metabolism*
  • DNA-Binding Proteins / metabolism
  • DNA-Binding Proteins / physiology*
  • Fluorescence Polarization
  • Fluorescent Dyes
  • Kinetics
  • Nucleic Acid Conformation
  • Nucleic Acid Denaturation
  • Phase Transition*
  • Regulatory Sequences, Nucleic Acid*
  • Viral Proteins / metabolism
  • Viral Proteins / physiology*

Substances

  • DNA, Single-Stranded
  • DNA, Viral
  • DNA-Binding Proteins
  • Fluorescent Dyes
  • Viral Proteins
  • rep proteins, Adeno-associated virus 2
  • Adenosine Triphosphate
  • DNA Helicases