Surfactant-based methods for prevention of protein adsorption in capillary electrophoresis

Methods Mol Biol. 2004:276:1-14. doi: 10.1385/1-59259-798-X:001.

Abstract

Surfactants such as didodecyldimethyl ammonium bromide (DDAB) and 1,2-dilauroyl-sn-phosphatidylcholine (DLPC) form bilayers at the walls of bare silica capillaries. Once formed, these bilayers are stable in the absence of surfactant in the buffer. DDAB provides a cationic bilayer coating which yields a strong reversed EOF and is effective for separation of cationic proteins. DLPC provides a zwitterionic bilayer coating which is effective for both cationic and anionic proteins. The electroosmotic flow (EOF) is strongly suppressed in DLPC-coated capillaries, thus low mobility proteins are slow to elute, and so the coating is favored for separation of high mobility proteins.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adsorption
  • Electrophoresis, Capillary
  • Phosphatidylcholines / chemistry*
  • Proteins / chemistry*
  • Quaternary Ammonium Compounds / chemistry*
  • Surface-Active Agents / chemistry*

Substances

  • Phosphatidylcholines
  • Proteins
  • Quaternary Ammonium Compounds
  • Surface-Active Agents
  • didodecyldimethylammonium
  • 1,2-dilauroylphosphatidylcholine