Synthesis of the thapsigargins

Proc Natl Acad Sci U S A. 2004 Aug 17;101(33):12073-8. doi: 10.1073/pnas.0403300101. Epub 2004 Jun 28.

Abstract

The thapsigargins are a family of complex guaianolides with potent and selective Ca(2+)-modulating properties. This article documents the evolution of a synthetic route through several iterations to a final practical and scaleable synthetic route capable of generating both unnatural and natural products based around the guaianolide skeleton.

MeSH terms

  • Apiaceae / chemistry
  • Biological Products / chemical synthesis
  • Biological Products / chemistry
  • Chemistry, Organic / methods
  • Molecular Structure
  • Stereoisomerism
  • Thapsigargin / analogs & derivatives*
  • Thapsigargin / chemical synthesis
  • Thapsigargin / chemistry

Substances

  • Biological Products
  • Thapsigargin