Caged phosphopeptides reveal a temporal role for 14-3-3 in G1 arrest and S-phase checkpoint function

Nat Biotechnol. 2004 Aug;22(8):993-1000. doi: 10.1038/nbt997. Epub 2004 Jul 25.

Abstract

Using classical genetics to study modular phosphopeptide-binding domains within a family of proteins that are functionally redundant is difficult when other members of the domain family compensate for the product of the knocked-out gene. Here we describe a chemical genetics approach that overcomes this limitation by using UV-activatable caged phosphopeptides. By incorporating a caged phosphoserine residue within a consensus motif, these reagents simultaneously and synchronously inactivate all phosphoserine/phosphothreonine-binding domain family members in a rapid and temporally regulated manner. We applied this approach to study the global function of 14-3-3 proteins in cell cycle control. Activation of the caged phosphopeptides by UV irradiation displaced endogenous proteins from 14-3-3-binding, causing premature cell cycle entry, release of G1 cells from interphase arrest and loss of the S-phase checkpoint after DNA damage, accompanied by high levels of cell death. This class of reagents will greatly facilitate molecular dissection of kinase-dependent signaling pathways when applied to other phosphopeptide-binding domains including SH2, Polo-box and tandem BRCT domains.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • 14-3-3 Proteins / metabolism*
  • Apoptosis
  • Cell Line, Tumor
  • Cell Survival
  • G1 Phase*
  • Humans
  • Osteosarcoma / metabolism*
  • Osteosarcoma / pathology*
  • Phosphopeptides / metabolism*
  • Phosphopeptides / radiation effects
  • Photochemistry / methods*
  • Recombinant Proteins / metabolism
  • Recombinant Proteins / radiation effects
  • S Phase*
  • Signal Transduction
  • Structure-Activity Relationship
  • Time Factors
  • Ultraviolet Rays

Substances

  • 14-3-3 Proteins
  • Phosphopeptides
  • Recombinant Proteins