A theoretical study of spin states in Ni-S4 complexes and models of the [NiFe] hydrogenase active site

J Biol Inorg Chem. 2004 Oct;9(7):873-84. doi: 10.1007/s00775-004-0588-2. Epub 2004 Sep 9.

Abstract

We have applied density functional theory, using both pure (BP86) and hybrid (B3LYP and B3LYP*) functionals, to investigate structural parameters and reaction energies for nickel(II)-sulfur coordination compounds, as well as for small cluster models of the Ni-SI and Ni-R redox state of [NiFe] hydrogenases. Results obtained investigating experimentally well-characterized complexes show that BP86 is well suited to describe the structural features of this class of compounds. However, the singlet-triplet energy splitting and even the computed ground state are strongly dependent on the applied functional. Results for the cluster models of [NiFe] hydrogenases lead to the conclusion that in the reduced protein structures characterized by X-ray diffraction a hydride bridges the two metal centres. The energy splitting of the singlet and triplet states in Ni-R and Ni-SI models is calculated to be very small and may be overcome at room temperature to allow a spin crossover. Moreover, the relative stability of the Ni-SI and Ni-R structures adopted in the present investigation is fully compatible with their involvement in the reversible heterolytic cleavage of H(2).

MeSH terms

  • Binding Sites
  • Desulfovibrio gigas / enzymology
  • Hydrogenase / chemistry*
  • Hydrogenase / metabolism
  • Models, Molecular
  • Molecular Conformation
  • Molecular Structure
  • Nickel / chemistry*
  • Oxidation-Reduction
  • Sulfur / chemistry*

Substances

  • Sulfur
  • Nickel
  • nickel-iron hydrogenase
  • Hydrogenase