Characterization of an RNA bulge structure by Fourier transform infrared spectroscopy

Biochem Biophys Res Commun. 2004 Nov 12;324(2):634-9. doi: 10.1016/j.bbrc.2004.09.098.

Abstract

There may be several advantages associated with an antisense oligonucleotide that induces a bulged structure into its RNA target molecule. Many structures of RNA bulges are elucidated from single-stranded RNA models. However, a two-component system is the minimum requirement for a realistic antisense model. We have used Fourier transform infrared spectroscopy to investigate a single-stranded RNA oligonucleotide with known NMR solution structure, constructed to model a five nucleotide bulge, and its two-component oligonucleotide counterpart. The infrared spectra show A-helical base-paired stems and non-base-paired loops in both systems. The nucleosides are mainly in an anti-conformation. Both N-type and S-type of sugar puckers can be inferred from the infrared region sensitive to sugar conformations. The S-type of sugar pucker is likely to be associated with the nucleotides in the bulge. The FTIR results display an overall structural similarity between the two model systems.

MeSH terms

  • Base Sequence
  • Carbohydrates / chemistry
  • Chromatography, High Pressure Liquid
  • Magnetic Resonance Spectroscopy
  • Molecular Sequence Data
  • Nucleic Acid Conformation*
  • Oligonucleotides, Antisense / chemistry
  • Phosphates / chemistry
  • RNA / chemistry*
  • Spectroscopy, Fourier Transform Infrared / methods*

Substances

  • Carbohydrates
  • Oligonucleotides, Antisense
  • Phosphates
  • RNA