[Study on determination of polycholorinated biphenyls in fish by isotopedilution GC-LRMS]

Jing-Guang Li; Yong-Ning Wu

[Study on determination of polycholorinated biphenyls in fish by isotopedilution GC-LRMS]

Wei Sheng Yan Jiu. 2005 May;34(3):322-5.

[Article in Chinese]

Authors

Jing-Guang Li¹, Yong-Ning Wu

Affiliation

¹ Institute of Nutrition and Food Safety, Chinese Center for Disease Control and Prevention, Beijing, China.

PMID: 16111042

Abstract

Objective: To develop a method for determination of 20 indicator polycholorinated biphenyls in fish by GC-LRMS.

Methods: Fish sample was added 13C lablled internal standard and cleaned-up by a multilayer silica column and a alumina column. Sample was analyzed by HRGC-LRMS using SIM mode.

Results: Detection limits of 20 indicator polycholorinated biphenyls were 0.009 - 0.044 ng/g. Average recovery were 79.7% - 112.6%, RSD were 1% - 8% (n = 6).

Conclusion: Results showed that the method was suitable for determination of indicator PCB in fish sample.

Publication types

English Abstract
Research Support, Non-U.S. Gov't

MeSH terms

Animals
Fishes / metabolism*
Food Contamination / analysis*
Gas Chromatography-Mass Spectrometry / methods*
Polychlorinated Biphenyls / analysis*
Radioisotope Dilution Technique

Substances

Polychlorinated Biphenyls