Correlation of temperature induced conformation change with optimum catalytic activity in the recombinant G/11 xylanase A from Bacillus subtilis strain 168 (1A1)

FEBS Lett. 2005 Nov 21;579(28):6505-10. doi: 10.1016/j.febslet.2005.10.039. Epub 2005 Nov 2.

Abstract

The 1.7A resolution crystal structure of recombinant family G/11 beta-1,4-xylanase (rXynA) from Bacillus subtilis 1A1 shows a jellyroll fold in which two curved beta-sheets form the active-site and substrate-binding cleft. The onset of thermal denaturation of rXynA occurs at 328 K, in excellent agreement with the optimum catalytic temperature. Molecular dynamics simulations at temperatures of 298-328 K demonstrate that below the optimum temperature the thumb loop and palm domain adopt a closed conformation. However, at 328 K these two domains separate facilitating substrate access to the active-site pocket, thereby accounting for the optimum catalytic temperature of the rXynA.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacillus subtilis / enzymology*
  • Binding Sites
  • Catalysis
  • Crystallography
  • Endo-1,4-beta Xylanases / chemistry*
  • Hot Temperature*
  • Molecular Sequence Data
  • Protein Conformation
  • Protein Denaturation
  • Recombinant Proteins / chemistry
  • Temperature

Substances

  • Recombinant Proteins
  • Endo-1,4-beta Xylanases