Expression of human cationic trypsinogen with an authentic N terminus using intein-mediated splicing in aminopeptidase P deficient Escherichia coli

Protein Expr Purif. 2006 Jul;48(1):104-11. doi: 10.1016/j.pep.2006.01.023. Epub 2006 Feb 21.

Abstract

High-level expression of human trypsinogens as inclusion bodies in Escherichia coli requires deletion of the secretory signal sequence and placement of an initiator methionine at the N terminus. Trypsinogen preparations obtained this way contain a mixture of abnormal N termini, as a result of processing by cytoplasmic aminopeptidases. Here, we describe an expression system that produces recombinant human cationic trypsinogen with a native, intact N terminus, using intein-mediated protein splicing and an aminopeptidase P (pepP) deficient E. coli strain. As a first application of this system, the effect of the pancreatitis-associated mutation A16V on the autoactivation of human cationic trypsinogen was characterized. The use of the novel pepP knock-out E. coli strain should be generally applicable to the expression of recombinant proteins, which undergo unwanted N-terminal trimming by aminopeptidase P.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Aminopeptidases / genetics
  • Aminopeptidases / metabolism
  • Base Sequence
  • Enzyme Activation
  • Escherichia coli / genetics*
  • Escherichia coli / metabolism
  • Humans
  • Inteins*
  • Molecular Sequence Data
  • Mutation
  • Protein Splicing*
  • Recombinant Fusion Proteins / genetics
  • Recombinant Fusion Proteins / metabolism
  • Recombinant Proteins / genetics
  • Recombinant Proteins / metabolism
  • Sequence Deletion
  • Trypsin
  • Trypsinogen / genetics*
  • Trypsinogen / isolation & purification
  • Trypsinogen / metabolism

Substances

  • Recombinant Fusion Proteins
  • Recombinant Proteins
  • Trypsinogen
  • Aminopeptidases
  • X-Pro aminopeptidase
  • PRSS1 protein, human
  • Trypsin