[Preparation of 10-hydroxycamptothecin semisolid lipid nanoparticles and investigation of its stability]

Zhong Yao Cai. 2006 Jan;29(1):63-6.
[Article in Chinese]

Abstract

Objective: To prepare 10-hydroxycamptothecin-semisolid lipid nanoparticles (HCPT-SSLN) and investigate its stability.

Methods: HCPT-SSLN was prepared by the method of "emulsion evaporation at a high temperature and solidification at a low temperature"; The morphology was examined by transmission electron microscope; The particle size and xi potential were determined by laser granularity equipment; The physical stability of both suspl and freeze drying powder of HCPT-SSLN were investigated.

Results: The mean particle size of the prepared HCPT-SSLN was 130.5 nm, drug loading was 2.51%, entrapment efficiency was 79.19%, xi potential was -33.1 mV; Placed at room temperature and 4 degrees C for 6 months, the appearance, particle size and entrapment efficiency of HCPT-SSLN were all stable. Moreover, the freeze drying powder was more stable than the suspl.

Conclusion: The HCPT-SSLN has high entrapment efficiency and drug loading, uniform particle size, good stability, which initially indicates that HCPT is fit for being incorporated into SSLN.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antineoplastic Agents, Phytogenic / chemistry*
  • Camptothecin / analogs & derivatives*
  • Camptothecin / analysis
  • Camptothecin / chemistry
  • Drug Carriers
  • Drug Stability
  • Freeze Drying
  • Lipids
  • Nanostructures
  • Particle Size
  • Polymers / chemistry
  • Powders
  • Technology, Pharmaceutical / methods*

Substances

  • Antineoplastic Agents, Phytogenic
  • Drug Carriers
  • Lipids
  • Polymers
  • Powders
  • 10-hydroxycamptothecin
  • Camptothecin