Development of a purge and trap continuous flow system for the stable carbon isotope analysis of volatile halogenated organic compounds in water

J Chromatogr A. 2006 Oct 27;1131(1-2):24-36. doi: 10.1016/j.chroma.2006.07.043. Epub 2006 Aug 8.

Abstract

A purge and trap (P&T) continuous flow system was developed in order to concentrate high volumes of water for trace analyses and stable carbon isotope measurements of volatile halogenated organic compounds (VHOCs) in seawater. The P&T parameters were evaluated regarding quality parameters, extraction efficiency and isotope fractionation. Precision (about 20%), linearity (>0.9676), and recoveries (between 75% and 99%) were reasonable within the large concentration range tested. Isotope fractionation was between 1 per thousand and 3 per thousand. Finally, the developed system was successfully applied to the quantitative and stable carbon isotope analysis of three water samples of different origin.

MeSH terms

  • Carbon Isotopes / analysis
  • Chromatography, Gas / instrumentation
  • Chromatography, Gas / methods*
  • Hydrocarbons, Halogenated / analysis*
  • Hydrocarbons, Halogenated / chemistry
  • Reproducibility of Results
  • Volatilization
  • Water / analysis*
  • Water / chemistry

Substances

  • Carbon Isotopes
  • Hydrocarbons, Halogenated
  • Water