Purification of a stilbene sensitive chloride channel and reconstitution of chloride conductivity into phospholipid vesicles

Biochem Biophys Res Commun. 1990 Sep 28;171(3):920-5. doi: 10.1016/0006-291x(90)90771-e.

Abstract

A protein conferring passive chloride permeability was isolated from a N-octylglucoside solubilized extract of partially purified H(+)-transporting osteoclast cell membranes. Purification was achieved by binding of solubilized protein to an amine-linked 4,4'-diisothiocyanatostilbene-2,2'-disulfonate (DIDS) Sepharose 4B column and elution with 50 mM KCl. A major protein, with MR = 60 kD on 10% SDS-PAGE, was obtained, which was further purified to homogeneity by HPLC gel filtration. This protein introduced 36Cl- permeability when reconstituted in phospholipid membranes by equilibrium dialysis. The Cl- transport recovered in reconstituted membranes retained sensitivity to DIDS confirming the identity of the isolated protein as a stilbene-sensitive chloride channel.

MeSH terms

  • 4,4'-Diisothiocyanostilbene-2,2'-Disulfonic Acid
  • 4-Acetamido-4'-isothiocyanatostilbene-2,2'-disulfonic Acid / analogs & derivatives
  • Animals
  • Cell Membrane / physiology
  • Chickens
  • Chloride Channels
  • Chlorides / metabolism
  • Chromatography, Affinity
  • Chromatography, Gel
  • Female
  • Ion Channels / drug effects
  • Ion Channels / physiology*
  • Ion Channels / ultrastructure
  • Liposomes*
  • Membrane Proteins / isolation & purification
  • Membrane Proteins / physiology*
  • Microscopy, Electron
  • Osteoclasts / physiology*
  • Stilbenes / pharmacology*

Substances

  • Chloride Channels
  • Chlorides
  • Ion Channels
  • Liposomes
  • Membrane Proteins
  • Stilbenes
  • 4-Acetamido-4'-isothiocyanatostilbene-2,2'-disulfonic Acid
  • 4,4'-Diisothiocyanostilbene-2,2'-Disulfonic Acid