Elucidation of human choline kinase crystal structures in complex with the products ADP or phosphocholine

J Mol Biol. 2006 Nov 24;364(2):136-51. doi: 10.1016/j.jmb.2006.08.084. Epub 2006 Sep 3.

Abstract

Choline kinase, responsible for the phosphorylation of choline to phosphocholine as the first step of the CDP-choline pathway for the biosynthesis of phosphatidylcholine, has been recognized as a new target for anticancer therapy. Crystal structures of human choline kinase in its apo, ADP and phosphocholine-bound complexes, respectively, reveal the molecular details of the substrate binding sites. ATP binds in a cavity where residues from both the N and C-terminal lobes contribute to form a cleft, while the choline-binding site constitutes a deep hydrophobic groove in the C-terminal domain with a rim composed of negatively charged residues. Upon binding of choline, the enzyme undergoes conformational changes independently affecting the N-terminal domain and the ATP-binding loop. From this structural analysis and comparison with other kinases, and from mutagenesis data on the homologous Caenorhabditis elegans choline kinase, a model of the ternary ADP.phosphocholine complex was built that reveals the molecular basis for the phosphoryl transfer activity of this enzyme.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adenosine Diphosphate / chemistry*
  • Adenosine Triphosphate / chemistry
  • Amino Acid Sequence
  • Binding Sites
  • Caenorhabditis elegans Proteins / chemistry
  • Choline / chemistry*
  • Choline Kinase / chemistry*
  • Crystallography, X-Ray
  • Humans
  • Hydrophobic and Hydrophilic Interactions
  • Models, Molecular*
  • Molecular Sequence Data
  • Phosphorylcholine / chemistry*
  • Protein Conformation
  • Sequence Homology, Amino Acid
  • Substrate Specificity

Substances

  • Caenorhabditis elegans Proteins
  • Phosphorylcholine
  • Adenosine Diphosphate
  • Adenosine Triphosphate
  • Choline Kinase
  • Choline

Associated data

  • PDB/2CKO
  • PDB/2CKP
  • PDB/2CKQ