Targeting Beta-3 integrin using a linear hexapeptide labeled with a near-infrared fluorescent molecular probe

Mol Pharm. 2006 Sep-Oct;3(5):539-49. doi: 10.1021/mp0600642.

Abstract

Biomolecules containing the RGD peptide sequence are known to bind integrins with high affinity. Studies of hexa-and hepta-peptides labeled with a near-infrared fluorescent probe (cypate) showed that rearranging the glycine in a linear RGD peptide sequence to form the GRD analogue favored the uptake of the GRD compound by alphavbeta3 integrin receptor (ABIR)-positive A549 tumor cells and tissue. The internalization of the GRD compound in A549 cells and tumor uptake in mice were inhibited by ABIR-avid peptides, suggesting its recognition by this receptor. Further studies with functional blocking antibodies and beta3 knockout cells revealed that beta3 integrin mediates the internalization of the cypate-GRD peptide. Molecular modeling studies supported preferential interaction of the probe with the beta3 subunit of integrins relative to the alphav subunit. The results demonstrate that the cypate-GRD peptide targets beta3 integrin, thereby providing a strategy to monitor drug delivery and efficacy, and physiopathologic processes mediated by this protein.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Animals
  • Binding, Competitive
  • Blotting, Western
  • Cell Line
  • Cell Line, Tumor
  • Fluorescent Dyes / chemistry*
  • Humans
  • Integrin beta Chains / genetics
  • Integrin beta Chains / metabolism*
  • Mice
  • Mice, Nude
  • Microscopy, Confocal
  • Molecular Probes / chemistry*
  • Molecular Structure
  • Muscle, Smooth, Vascular / cytology
  • Muscle, Smooth, Vascular / drug effects
  • Muscle, Smooth, Vascular / metabolism
  • Mutation
  • Oligopeptides / chemistry
  • Oligopeptides / metabolism
  • Oligopeptides / pharmacology*
  • Spectroscopy, Near-Infrared / methods
  • Time Factors
  • Xenograft Model Antitumor Assays

Substances

  • Fluorescent Dyes
  • Integrin beta Chains
  • Molecular Probes
  • Oligopeptides
  • arginyl-glycyl-aspartic acid