2-methoxyestradiol, an endogenous mammalian metabolite, radiosensitizes colon carcinoma cells through c-Jun NH2-terminal kinase activation

Clin Cancer Res. 2006 Nov 1;12(21):6532-9. doi: 10.1158/1078-0432.CCR-06-0678.

Abstract

Purpose: 2-Methoxyestradiol (2ME), an estrogen metabolite, induces apoptosis in various cell types. We investigated whether 2ME pretreatment can radiosensitize colon adenocarcinoma cells.

Experimental design: Radiosensitizing effects of 2ME were evaluated by cell death, clonogenic assay, nuclear fragmentation, and tumor progression of xenografts. Ionizing radiation-induced DNA damage was evaluated by histone H2AX phosphorylation and its foci. The c-Jun NH2-terminal kinase (JNK) activation was evaluated by anti-phosphorylated JNK antibody and inhibited by the JNK-specific inhibitor SP600125 or dominant-negative SEK1 expression.

Results: Clonogenic assays revealed that 2ME, but not estradiol, radiosensitized three colon carcinoma cells, DLD-1, HCT-8, and HCT-15, and strongly suppressed tumor progression of DLD-1 xenografts. Gene transfer-mediated Bcl-xL overexpression largely abolished both augmented apoptosis and reduced survival fractions. Pretreatment with 2ME enhanced H2AX phosphorylation, its foci, and phosphorylation of ATM kinase and delayed re-entry of cell cycle progression after ionizing radiation. Augmentation of both radiosensitivity and H2AX phosphorylation was substantially reduced by SP600125 or overexpression of a dominant-negative mutant SEK1.

Conclusion: 2ME radiosensitized colon carcinoma cells through enhanced DNA damage via JNK activation, thereby representing a novel radiosensitizing therapy against colon cancer.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • 2-Methoxyestradiol
  • Adenocarcinoma / therapy*
  • Animals
  • Apoptosis / physiology
  • Blotting, Western
  • Cell Cycle / radiation effects
  • Cell Line, Tumor
  • Colonic Neoplasms / therapy*
  • Combined Modality Therapy
  • DNA Damage / radiation effects
  • Estradiol / analogs & derivatives*
  • Estradiol / metabolism
  • Estradiol / pharmacokinetics
  • Histones / metabolism
  • Humans
  • JNK Mitogen-Activated Protein Kinases / drug effects
  • JNK Mitogen-Activated Protein Kinases / metabolism*
  • Mice
  • Mice, Nude
  • Microscopy, Confocal
  • Phosphorylation
  • Radiation, Ionizing
  • Radiation-Sensitizing Agents / pharmacokinetics*
  • Transfection
  • Xenograft Model Antitumor Assays

Substances

  • H2AX protein, human
  • Histones
  • Radiation-Sensitizing Agents
  • Estradiol
  • 2-Methoxyestradiol
  • JNK Mitogen-Activated Protein Kinases