Crystallographic refinement of the three-dimensional structure of the FabD1.3-lysozyme complex at 2.5-A resolution

J Biol Chem. 1991 Jul 15;266(20):12915-20.

Abstract

The three-dimensional crystal structure of the complex between the Fab from the monoclonal anti-lysozyme antibody D1.3 and the antigen, hen egg white lysozyme, has been refined by crystallographic techniques using x-ray intensity data to 2.5-A resolution. The antibody contacts the antigen with residues from all its complementarity determining regions. Antigen residues 18-27 and 117-125 form a discontinuous antigenic determinant making hydrogen bonds and van der Waals interactions with the antibody. Water molecules at or near the antigen-antibody interface mediate some contacts between antigen and antibody. The fine specificity of antibody D1.3, which does not bind (K alpha less than 10(5) M-1) avian lysozymes where Gln121 in the amino acid sequence is occupied by His, can be explained on the basis of the refined model.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Antibodies, Monoclonal*
  • Binding Sites, Antibody
  • Epitopes / chemistry
  • Immunoglobulin Fab Fragments*
  • Models, Molecular
  • Molecular Sequence Data
  • Muramidase / chemistry
  • Muramidase / immunology*
  • Protein Conformation
  • X-Ray Diffraction / methods

Substances

  • Antibodies, Monoclonal
  • Epitopes
  • Immunoglobulin Fab Fragments
  • Muramidase