The synthesis of 1-thia-6-oxa-6alambda(4)-seleno-3-azapentalene and a 3H-1,2,4-dithiazole

Org Biomol Chem. 2007 Feb 21;5(4):613-6. doi: 10.1039/b617097h. Epub 2007 Jan 12.

Abstract

The reaction of thiocarbamoyl isoselenocyanate with a carbanion gave 1-thia-6-oxa-6alambda(4)-seleno-3-azapentalene, which has a hypervalent selenium, as the major product. The by-products 3-diacylmethylidene-5-dimethylamino-3H-1,2,4-dithiazole and thiocarbamate thioanhydride were also formed.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bridged Bicyclo Compounds, Heterocyclic / chemical synthesis*
  • Bridged Bicyclo Compounds, Heterocyclic / chemistry
  • Magnetic Resonance Spectroscopy / methods
  • Models, Molecular
  • Molecular Structure
  • Organoselenium Compounds / chemical synthesis*
  • Organoselenium Compounds / chemistry
  • Sensitivity and Specificity
  • Stereoisomerism
  • Thiazoles / chemical synthesis*
  • Thiazoles / chemistry
  • Thiocarbamates / chemical synthesis
  • Thiocarbamates / chemistry

Substances

  • 1-thia-6-oxa-6agamma(4)-seleno-3-azapentalene
  • Bridged Bicyclo Compounds, Heterocyclic
  • Organoselenium Compounds
  • Thiazoles
  • Thiocarbamates