Urinary hydroxylated metabolites of polycyclic aromatic hydrocarbons as biomarkers of exposure in asphalt workers

Biomarkers. 2007 May-Jun;12(3):221-39. doi: 10.1080/13547500601100110.

Abstract

Background: Fumes and vapours released during laying of hot asphalt mix have been recognised as a major source of exposure for asphalt workers.

Objectives: We investigated the relationships between inhalation exposure to asphalt emissions and urinary biomarkers of polycyclic aromatic hydrocarbons (PAHs) in asphalt workers (AW, n=75) and in ground construction workers (CW, n=37).

Methods: Total polyaromatic compounds (PAC) and 15 priority PAHs in inhaled air were measured by personal sampling. Hydroxylated PAH metabolites (OH-PAHs) (2-naphthol, 2-hydroxyfluorene, 3-hydroxyphenanthrene, 1-hydroxypyrene, 6-hydroxychrysene and 3-hydroxybenzo[a]pyrene) were determined in urine spot samples collected in three different times during the work week.

Results: Median vapour-phase PAC (5.5 microg m(-3)), PAHs (<or=50 ng m(-3)) and OH-PAHs (0.08-1.11 microg l(-1)) were significantly higher in AW than in CW, except in the cases of air naphthalene and 2-naphthol. Airborne levels of particle-phase contaminants were similar in the two groups and much lower than vapour-phase levels; metabolites of particulate PAHs were never found in quantifiable amounts. An appreciable increase in OH-PAH levels during the work day and work week was found in AW; median levels for 2-hydroxyfluorene, 3-hydroxyphenanthrene and 1-hydroxypyrene were, respectively, 0.29, 0.08 and 0.18 at baseline; 0.50, 0.18 and 0.29, pre-shift; 1.11, 0.44 and 0.44 microg l(-1), post-shift. Each OH-PAH exhibited a characteristic profile of increase, reflecting differences in half-lives of the parent compounds. In non-smoking subjects, positive correlations were found between vapour-phase PAC or PAHs and OH-PAHs both in pre- and post-shift samples (0.34 <or= r<or=69). Smokers exhibited 2-5-fold higher OH-PAHs than non-smokers, at any time and at both workplaces.

Conclusions: Our results suggest that OH-PAHs are useful biomarkers for monitoring exposure to asphalt emissions. The work-related exposure to PAC and PAHs was low in all AW, but urinary metabolites reflected exposure satisfactorily.

MeSH terms

  • Adult
  • Aged
  • Air / analysis
  • Air Pollutants, Occupational / analysis*
  • Benzopyrenes / analysis
  • Biomarkers / urine*
  • Chrysenes / urine
  • Environmental Monitoring / methods
  • Fluorenes / urine
  • Humans
  • Hydrocarbons*
  • Hydroxylation
  • Inhalation Exposure
  • Italy
  • Male
  • Middle Aged
  • Naphthols / urine
  • Occupational Exposure / analysis*
  • Phenanthrenes / urine
  • Polycyclic Aromatic Hydrocarbons / metabolism
  • Polycyclic Aromatic Hydrocarbons / urine*
  • Pyrenes / analysis
  • Smoking / urine

Substances

  • Air Pollutants, Occupational
  • Benzopyrenes
  • Biomarkers
  • Chrysenes
  • Fluorenes
  • Hydrocarbons
  • Naphthols
  • Phenanthrenes
  • Polycyclic Aromatic Hydrocarbons
  • Pyrenes
  • 6-hydroxychrysene
  • 3-hydroxybenzo(a)pyrene
  • asphalt
  • 2-hydroxyfluorene
  • 1-hydroxypyrene
  • 2-naphthol