Developing chiral ligands for asymmetric hydrogenation

Acc Chem Res. 2007 Dec;40(12):1278-90. doi: 10.1021/ar7000028. Epub 2007 May 17.

Abstract

This Account outlines our efforts in ligand development for asymmetric hydrogenation. The successful development of three classes of ligands is presented, including (1) ligands with phosphocyclic motifs, (2) ligands with atropisomeric backbones, and (3) bisphosphine ligands inspired by the structure of 2,3- O-isopropylidene-2,3-dihydroxyl-1,4-bis(diphenylphosphino)butane (DIOP). With this large ligand toolbox, we have prepared many pharmaceutically valuable chiral products efficiently.

Publication types

  • Research Support, N.I.H., Extramural
  • Review

MeSH terms

  • Butanes / chemistry*
  • Hydrogenation
  • Ligands
  • Phosphines / chemistry*
  • Rhodium / chemistry
  • Stereoisomerism

Substances

  • 2,3- O-isopropylidene-2,3-dihydroxyl-1,4-bis(diphenylphosphino)butane
  • Butanes
  • Ligands
  • Phosphines
  • Rhodium
  • phosphine