Stereoselective olefin isomerization leading to asymmetric quaternary carbon construction

Org Lett. 2007 Jun 7;9(12):2325-8. doi: 10.1021/ol0706511. Epub 2007 May 17.

Abstract

Chemo- and stereoselective Ir(I)-catalyzed isomerization of 1,1-disubstituted and trisubstituted allylic ethers and in situ [3,3] sigmatropic rearrangement of the resulting allyl vinyl ethers provide for the highly stereoselective construction of quaternary carbon stereocenters. The olefin isomerization-Claisen rearrangement (ICR) sequence allows adjacent quaternary-tertiary stereocenter relationships to be established with excellent diastereoselection. Several complementary strategies for enantioselective quaternary carbon synthesis derive directly from the ICR reaction design.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Alkenes / chemical synthesis
  • Alkenes / chemistry*
  • Molecular Conformation
  • Stereoisomerism

Substances

  • Alkenes