A novel flavonoid from Lespedeza virgata (Thunb.) DC.: structural elucidation and antioxidative activity

Bioorg Med Chem Lett. 2007 Nov 15;17(22):6311-5. doi: 10.1016/j.bmcl.2007.09.003. Epub 2007 Sep 7.

Abstract

Bioactivity guided fractionation of the ethanolic extract of the whole plants of Lespedeza virgata (Thunb.) DC. resulted in the isolation of a novel flavonoid (1) along with five known compounds 2-6. The molecular and structural formula as well as the stereochemistry of compound 1 were determined using data obtained from (1)H and (13)C NMR spectra, DEPT135 and by 2D HSQC, HMBC, (1)H-(1)H correlated spectroscopy ((1)H-(1)H COSY), and nuclear overhauser effect spectroscopy (NOESY) experiments. The superoxide anion scavenging activities of all isolated compounds were evaluated by the hypoxanthine nitro blue tetrazolium and ESR methods and the new compound 1 showed the strongest antioxidative activity 95.79% (IC(50)=0.14 mg/ml).

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antioxidants / chemistry*
  • Antioxidants / isolation & purification
  • Electron Spin Resonance Spectroscopy
  • Ethanol / chemistry
  • Flavonoids / chemistry*
  • Flavonoids / isolation & purification
  • Inhibitory Concentration 50
  • Lespedeza / chemistry*
  • Magnetic Resonance Spectroscopy
  • Molecular Structure
  • Solvents / chemistry
  • Superoxides / chemistry

Substances

  • Antioxidants
  • Flavonoids
  • Solvents
  • Superoxides
  • Ethanol