The structural basis of calcium transport by the calcium pump

Nature. 2007 Dec 13;450(7172):1036-42. doi: 10.1038/nature06418.

Abstract

The sarcoplasmic reticulum Ca2+-ATPase, a P-type ATPase, has a critical role in muscle function and metabolism. Here we present functional studies and three new crystal structures of the rabbit skeletal muscle Ca2+-ATPase, representing the phosphoenzyme intermediates associated with Ca2+ binding, Ca2+ translocation and dephosphorylation, that are based on complexes with a functional ATP analogue, beryllium fluoride and aluminium fluoride, respectively. The structures complete the cycle of nucleotide binding and cation transport of Ca2+-ATPase. Phosphorylation of the enzyme triggers the onset of a conformational change that leads to the opening of a luminal exit pathway defined by the transmembrane segments M1 through M6, which represent the canonical membrane domain of P-type pumps. Ca2+ release is promoted by translocation of the M4 helix, exposing Glu 309, Glu 771 and Asn 796 to the lumen. The mechanism explains how P-type ATPases are able to form the steep electrochemical gradients required for key functions in eukaryotic cells.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adenosine Triphosphate / metabolism
  • Animals
  • Beryllium
  • Calcium / metabolism*
  • Crystallography, X-Ray
  • Fluorides
  • Ion Transport
  • Mass Spectrometry
  • Models, Molecular
  • Muscle, Skeletal / enzymology
  • Muscle, Skeletal / metabolism
  • Phosphorylation
  • Protein Conformation
  • Rabbits
  • Sarcoplasmic Reticulum Calcium-Transporting ATPases / chemistry*
  • Sarcoplasmic Reticulum Calcium-Transporting ATPases / metabolism*
  • Structure-Activity Relationship
  • Thapsigargin

Substances

  • beryllium fluoride
  • Thapsigargin
  • Adenosine Triphosphate
  • Sarcoplasmic Reticulum Calcium-Transporting ATPases
  • Beryllium
  • Fluorides
  • Calcium

Associated data

  • PDB/3B9B
  • PDB/3B9R
  • PDB/3BA6