[Research on method in avoiding the interference of poloxamer in determination of polysaccharides in thermosensitive gel]

Zhong Yao Cai. 2007 Nov;30(11):1443-6.
[Article in Chinese]

Abstract

Objective: To study a method in avoiding the interference of poloxamer in determination of polysaccharides in thermosensitive gel and develop an assay correspondingly.

Methods: After extracting the freeze dried gel with acetic ether, detected it in colorimetric method.

Results: The interference of poloxamer was removed thoroughly, while the retention rate of the polysacchrarides showed to be 100.11% (n = 3). The average recovery was 102.6% (n = 6).

Conclusion: The method shows to be simple, maneuverable, stable and well reproducible.

Publication types

  • English Abstract
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Colorimetry / methods
  • Drugs, Chinese Herbal / chemistry*
  • Freeze Drying
  • Gels
  • Plants, Medicinal / chemistry
  • Poloxamer / chemistry*
  • Polysaccharides / analysis*
  • Polysaccharides / isolation & purification
  • Prunella / chemistry*
  • Quality Control
  • Reproducibility of Results
  • Solubility
  • Temperature

Substances

  • Drugs, Chinese Herbal
  • Gels
  • Polysaccharides
  • Poloxamer