Abstract
The Escherichia coli fumarate and nitrate reductase (FNR) regulator protein is an important transcriptional regulator that controls the expression of a large regulon of more than 100 genes in response to changes in oxygen availability. FNR is active when it acquires a [4Fe-4S](2+) cluster under anaerobic conditions. The presence of the [4Fe-4S](2+) cluster promotes protein dimerization and site-specific DNA binding, facilitating activation or repression of target promoters. Oxygen is sensed by the controlled disassembly of the [4Fe-4S](2+) cluster, ultimately resulting in inactive, monomeric, apo-FNR. The FNR [4Fe-4S](2+) cluster is also sensitive to nitric oxide, such that under anaerobic conditions the protein is inactivated by nitrosylation of the iron-sulfur cluster, yielding a mixture of monomeric and dimeric dinitrosyl-iron cysteine species. This chapter describes some of the methods used to produce active [4Fe-4S] FNR protein and investigates the reaction of the [4Fe-4S](2+) cluster with nitric oxide and oxygen in vitro.
MeSH terms
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Acids / pharmacology
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Anaerobiosis / genetics
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Escherichia coli / enzymology*
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Escherichia coli / genetics
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Escherichia coli / growth & development*
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Escherichia coli / metabolism
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Escherichia coli Proteins / chemistry
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Escherichia coli Proteins / isolation & purification
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Escherichia coli Proteins / metabolism*
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Escherichia coli Proteins / physiology
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Fumarates / metabolism*
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Gene Expression Regulation, Bacterial
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Iron / metabolism
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Iron-Sulfur Proteins / chemistry
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Iron-Sulfur Proteins / isolation & purification
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Iron-Sulfur Proteins / metabolism*
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Iron-Sulfur Proteins / physiology
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Nitrates / metabolism*
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Nitric Oxide / metabolism*
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Oxidation-Reduction
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Oxygen / metabolism*
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Peroxides / analysis
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Recombinant Proteins / isolation & purification
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Spectrophotometry, Ultraviolet
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Sulfides / metabolism
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Superoxides / analysis
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Transcription, Genetic
Substances
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Acids
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Escherichia coli Proteins
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FNR protein, E coli
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Fumarates
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Iron-Sulfur Proteins
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Nitrates
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Peroxides
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Recombinant Proteins
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Sulfides
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Superoxides
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ferryl iron
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Nitric Oxide
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Iron
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Oxygen