Structure elucidation and complete NMR spectral assignments of four new diterpenoids from Smallantus sonchifolius

Magn Reson Chem. 2008 Aug;46(8):775-9. doi: 10.1002/mrc.2242.

Abstract

Four new diterpenoids, named smaditerpenic acid A-D, together with five known compounds, were isolated from the H(2)O extract of the leaves of Smallantus sonchifolius (yacon) cultivated in Liaoning, China and their structures were elucidated on the basis of one- and two-dimensional NMR (including (1)H, (13)C-NMR, (1)H-(1)H COSY, HSQC, TOCSY, HMBC, and ROESY), electrospray ionization mass spectrometry (ESI-MS), and chemical methods.

MeSH terms

  • Asteraceae / chemistry*
  • Asteraceae / growth & development
  • China
  • Diterpenes / chemistry
  • Diterpenes / isolation & purification*
  • Magnetic Resonance Spectroscopy*
  • Molecular Structure
  • Plant Leaves / chemistry
  • Spectrometry, Mass, Electrospray Ionization

Substances

  • Diterpenes