Analysis of non-heme iron in arachidonate 12-lipoxygenase of porcine leukocytes

Biochim Biophys Acta. 1991 Jul 9;1084(2):202-4.

Abstract

Arachidonate 12-lipoxygenase of porcine leukocytes, which was purified to homogeneity by immunoaffinity chromatography, was analyzed for iron content by atomic absorption spectrophotometry. The enzyme contained 0.70 +/- 0.09 g atom of iron per mol of enzyme (mean +/- S.D., n = 4). Inorganic iron, which was added to the enzyme solution as an internal standard, was recovered in almost 100% yield. Among various iron chelators tested, only 2,2'-dipyridyl at 1 mM inactivated the enzyme by 87%, but the enzyme was not reactivated by the addition of excess ferrous or ferric iron.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Arachidonate 12-Lipoxygenase / blood*
  • Arachidonate 12-Lipoxygenase / chemistry
  • Arachidonate 12-Lipoxygenase / isolation & purification
  • Iron / analysis*
  • Leukocytes / enzymology*
  • Spectrophotometry, Atomic
  • Swine

Substances

  • Iron
  • Arachidonate 12-Lipoxygenase