In vivo evaluation of injectable thermosensitive polymer with time-dependent LCST

J Biomed Mater Res A. 2009 Sep 15;90(4):1186-97. doi: 10.1002/jbm.a.32179.

Abstract

The focus of this study was to examine the biocompatibility, time-dependent LCST, and bioerodable properties of a copolymer system composed of NIPAAm, dimethyl-gamma-butyrolactone (DMBL), and acrylic acid (AAc). Sprague Dawley rats were subcutaneously injected with 25 wt % solutions of poly(NIPAAm-co-DMBL-co-AAc). At predetermined times, animals were sacrificed and polymer implants were recovered for characterization via 1H-NMR. In addition, polymer-contacting tissue sections were harvested and processed for histology. The biocompatibility of the implants was assessed by counting the number of fibroblasts and leukocytes present at the tissue-implant interface. The LCST data obtained from the in vivo implants was shown to agree with that of in vitro findings. Implant mass was shown to decrease after 4 days, indicating accelerated diffusion rates with increased implant swelling, hydrolytic degradation was confirmed with 1H-NMR measurements. The cellular presence at the copolymer implant-tissue interface was shown to return to that of normal tissue 30 days postimplantation, which suggests a normal wound healing response.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Animals
  • Biocompatible Materials / administration & dosage*
  • Cell Count
  • Diffusion
  • Fibroblasts / cytology
  • Hot Temperature
  • Hydrolysis
  • Implants, Experimental / standards*
  • Injections
  • Leukocytes / cytology
  • Materials Testing
  • Polymers / administration & dosage*
  • Rats
  • Rats, Sprague-Dawley
  • Time Factors
  • Wound Healing

Substances

  • Biocompatible Materials
  • Polymers