Molecular cloning, expression, and characterization of a novel endo-alpha-N-acetylgalactosaminidase from Enterococcus faecalis

Biochem Biophys Res Commun. 2008 Oct 31;375(4):441-6. doi: 10.1016/j.bbrc.2008.08.065. Epub 2008 Aug 24.

Abstract

We report here the molecular cloning, expression and characterization of a novel endo-alpha-N-acetylgalactosaminidase, classified into the GH101 family, from Enterococcus faecalis (endo-EF). The recombinant endo-EF was found to catalyze the liberation of core1-disaccharides (Galbeta1-3GalNAc) from core1-pNP (Galbeta1-3GalNAcalpha-pNP) like other GH101 family enzymes. However, endo-EF seems to differ in specificity from the GH101 enzymes reported to date, because it was able to release trisaccharides from core2-pNP (Galbeta1-3[GlcNAcbeta1-6]GalNAcalpha-pNP) and tetrasaccharides from Gal-core2-pNP (Galbeta1-3[Galbeta1-3GlcNAcbeta1-6]GalNAcalpha-pNP). Interestingly, the enzyme could transfer not only core1-disaccharides but also core2-trisaccharides to alkanols generating alkyl-oligosaccharides. Endo-EF should facilitate O-glycoprotein research.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Bacterial Proteins / biosynthesis
  • Bacterial Proteins / chemistry*
  • Bacterial Proteins / isolation & purification
  • Catalysis
  • Cloning, Molecular
  • Disaccharides / chemistry*
  • Enterococcus faecalis / enzymology*
  • Glycosylation
  • Molecular Sequence Data
  • Recombinant Proteins / biosynthesis
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / isolation & purification
  • Substrate Specificity
  • Trisaccharides / chemistry*
  • alpha-N-Acetylgalactosaminidase / biosynthesis
  • alpha-N-Acetylgalactosaminidase / chemistry*
  • alpha-N-Acetylgalactosaminidase / isolation & purification

Substances

  • Bacterial Proteins
  • Disaccharides
  • Recombinant Proteins
  • Trisaccharides
  • alpha-N-Acetylgalactosaminidase

Associated data

  • GENBANK/AB453240