Solution conformation of endothelin determined by means of 1H-NMR spectroscopy and distance geometry calculations

Protein Eng. 1991 Jun;4(5):509-18. doi: 10.1093/protein/4.5.509.

Abstract

The structure of endothelin-1 (ET-1), an endothelial cell-derived peptide with vasoconstricting activity, was determined in an aqueous solution by means of a combination of NMR and distance geometry calculations. The resulting structure is characterized by an alpha-helical conformation in the sequence region, Lys9-Cys15. Furthermore, an extended structure and a turn structure exist in the Cys1-Ser4 and Ser5-Asp8 regions respectively, and no preferred conformation was found for the C-terminal part of the peptide which was not uniquely constrained by the NMR data. These structural elements, the alpha-helical structure in the sequence portion, Cys-X-X-X-Cys, and the extended structure in Cys-X-Cys, are homologous to those found commonly in several neurotoxic peptides.

MeSH terms

  • Algorithms*
  • Amino Acid Sequence
  • Endothelins / chemistry*
  • Magnetic Resonance Spectroscopy*
  • Molecular Sequence Data
  • Molecular Weight
  • Protein Conformation
  • Sequence Homology, Nucleic Acid
  • Solutions
  • Structure-Activity Relationship

Substances

  • Endothelins
  • Solutions