Structural elucidation of four new furostanol saponins from Tupistra chinensis by 1D and 2D NMR spectroscopy

Kun Zou; Jun-zhi Wang; Zhi-yong Guo; Ming Du; Jun Wu; Yuan Zhou; Fei-jun Dan; Chuang Liu

doi:10.1002/mrc.2332

Structural elucidation of four new furostanol saponins from Tupistra chinensis by 1D and 2D NMR spectroscopy

Magn Reson Chem. 2009 Jan;47(1):87-91. doi: 10.1002/mrc.2332.

Authors

Kun Zou¹, Jun-zhi Wang, Zhi-yong Guo, Ming Du, Jun Wu, Yuan Zhou, Fei-jun Dan, Chuang Liu

Affiliation

¹ Hubei Key Laboratory of Natural Products Research and Development, College of Chemistry and Life Science, China Three Gorges University, Yichang 443002, PR China. [email protected]

PMID: 19003938
DOI: 10.1002/mrc.2332

Abstract

Four new furostanol saponins (1-4), two pairs of diastereoisomers, were isolated from methanolic extracts of Tupistra chinensis rhizomes and their structures were assigned from (1)H and (13)C NMR spectra, DEPT, and by 2D COSY, NOESY, HMQC, and HMBC experiments.

2008 John Wiley & Sons, Ltd.

Publication types

Research Support, Non-U.S. Gov't

MeSH terms

Magnetic Resonance Spectroscopy / methods*
Magnoliopsida / chemistry
Methanol
Molecular Structure
Plant Extracts / chemistry
Saponins / chemistry*
Stereoisomerism
Sterols / chemistry*

Substances

Plant Extracts
Saponins
Sterols
furostanol saponin I
Methanol