Synthesis and conformational analysis of cyclic analogues of inverse gamma-turns

Org Biomol Chem. 2008 Oct 7;6(19):3476-85. doi: 10.1039/b808954j. Epub 2008 Aug 7.

Abstract

Gamma-turn analogues comprising a modified dipeptide constrained in an eleven-membered ring were prepared by alkene metathesis and analysed by NMR and molecular modelling studies. The results reveal that some of the cyclic analogues form inverse gamma-turns and preferentially adopt conformations determined by the identity of the incorporated amino acid residues and the nature of the constraining linker (E/Z-alkene or alkane).

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkenes / chemistry
  • Carboxylic Acids / chemistry
  • Dipeptides / chemical synthesis
  • Dipeptides / chemistry*
  • Magnetic Resonance Spectroscopy
  • Models, Molecular
  • Molecular Conformation
  • Peptides, Cyclic / chemical synthesis
  • Peptides, Cyclic / chemistry*
  • Stereoisomerism

Substances

  • Alkenes
  • Carboxylic Acids
  • Dipeptides
  • Peptides, Cyclic