Capturing molecular structural dynamics by 100 ps time-resolved X-ray absorption spectroscopy

J Synchrotron Radiat. 2009 Jan;16(Pt 1):110-5. doi: 10.1107/S0909049508034596. Epub 2008 Nov 21.

Abstract

An experimental set-up for time-resolved X-ray absorption spectroscopy with 100 ps time resolution at beamline NW14A at the Photon Factory Advanced Ring is presented. The X-ray positional active feedback to crystals in a monochromator combined with a figure-of-merit scan of the laser beam position has been utilized as an essential tool to stabilize the spatial overlap of the X-ray and laser beams at the sample position. As a typical example, a time-resolved XAFS measurement of a photo-induced spin crossover reaction of the tris(1,10-phenanthrorine)iron(II) complex in water is presented.

Publication types

  • Research Support, Non-U.S. Gov't