Processing and properties of highly enriched double-wall carbon nanotubes

Nat Nanotechnol. 2009 Jan;4(1):64-70. doi: 10.1038/nnano.2008.364. Epub 2008 Dec 14.

Abstract

Carbon nanotubes consist of one or more concentric graphene cylinders and are under investigation for a variety of applications that make use of their excellent thermal, mechanical, electronic and optical properties. Double-wall nanotubes are ideal systems for studying the interwall interactions influencing the properties of nanotubes with two or more walls. However, current techniques to synthesize double-wall nanotubes produce unwanted single- and multiwall nanotubes. Here, we show how density gradient ultracentrifugation can be used to separate double-wall nanotubes from mixtures of single- and multiwall nanotubes through differences in their buoyant density. This technique results in samples that are highly enriched in either single- or double-wall nanotubes of similar outer wall diameter, with the double-wall nanotubes being, on average, approximately 44% longer than the single-wall nanotubes. The longer average length of the double-wall nanotubes provides distinct advantages when they are used in transparent conductors.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.