Significant steroids: effective and general synthesis of 4alpha- and 4beta-amino-5alpha-androstanes

Chem Commun (Camb). 2009 Mar 7:(9):1037-9. doi: 10.1039/b817910g. Epub 2009 Jan 27.

Abstract

4alpha-Aminosteroids were synthesized by the substitution of a 2alpha-bromo ketone using K(2)CO(3) as an activator; 4beta-aminosteroids were synthesized in excellent yields by a highly regioselective and trans-stereospecific ring opening of a steroidal 3,4alpha-epoxide using ZnCl(2)-H(2)O as a catalyst.

MeSH terms

  • Androstanes / chemical synthesis*
  • Androstanes / chemistry
  • Catalysis
  • Ketones / chemistry
  • Steroids / chemical synthesis*
  • Steroids / chemistry
  • Zinc / chemistry

Substances

  • Androstanes
  • Ketones
  • Steroids
  • Zinc