Definition of the affinity of binding between human von Willebrand factor and coagulation factor VIII

Biochem Biophys Res Commun. 1991 Oct 15;180(1):231-7. doi: 10.1016/s0006-291x(05)81281-1.

Abstract

Factor VIII and von Willebrand factor are two plasma proteins essential for effective hemostasis. In vivo, they form a non-covalent complex whose association appears to be metal ion dependent. However, a precise definition of the nature of the molecular forces governing their association remains to be defined, as does their binding affinity. In this paper we have determined the dissociation constant and stoichiometry for Factor VIII binding to immobilized von Willebrand factor. The data demonstrate that these proteins interact saturably and with relatively high affinity. Computer assisted analyses of the Scatchard data favour a two site binding model. The higher affinity site was found to have a Kd of 62 (+/- 13) x 10(-12) M while that of the lower affinity site was 380 (+/- 92) x 10(-12) M. The density of Factor VIII binding sites (Bmax) present on von Willebrand factor was 31 (+/- 3) pM for the high affinity binding site and 46 (+/- 6) pM for the lower site, corresponding to a calculated Factor VIII: von Willebrand factor binding ratio of 1:33 and 1:23, respectively.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Binding Sites
  • Electrophoresis, Polyacrylamide Gel
  • Enzyme-Linked Immunosorbent Assay
  • Factor VIII / chemistry*
  • Factor VIII / isolation & purification
  • Humans
  • Immunoblotting
  • Kinetics
  • Molecular Conformation
  • von Willebrand Factor / chemistry*
  • von Willebrand Factor / isolation & purification

Substances

  • von Willebrand Factor
  • Factor VIII