Fluorescence lifetime spectroscopy and imaging of nano-engineered glucose sensor microcapsules based on glucose/galactose-binding protein

Biosens Bioelectron. 2009 Jul 15;24(11):3229-34. doi: 10.1016/j.bios.2009.04.003. Epub 2009 Apr 14.

Abstract

We aimed to develop microsensors for eventual glucose monitoring in diabetes, based on fluorescence lifetime changes in glucose/galactose-binding protein (GBP) labelled with the environmentally sensitive fluorophore dye, badan. A mutant of GBP was labelled with badan near the binding site, the protein adsorbed to microparticles of CaCO(3) as templates and encapsulated in alternating nano-layers of poly-L-lysine and heparin. We used fluorescence lifetime imaging (FLIM) with two-photon excitation and time-correlated single-photon counting to visualize the lifetime changes in the capsules. Addition of glucose increased the mean lifetime of GBP-badan by a maximum of approximately 2 ns. Analysis of fluorescence decay curves was consistent with two GBP states, a short-lifetime component (approximately 0.8 ns), likely representing the open form of the protein with no bound glucose, and a long-lifetime component (approximately 3.1 ns) representing the closed form with bound glucose and where the lobes of GBP have closed round the dye creating a more hydrophobic environment. FLIM demonstrated that increasing glucose increased the fractional proportion of the long-lifetime component. We conclude that fluorescence lifetime-based glucose sensing using GBP encapsulated with nano-engineered layer-by-layer films is a glucose monitoring technology suitable for development in diabetes management.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biomedical Engineering / methods
  • Biosensing Techniques / methods*
  • Capsules
  • Enzyme Activation
  • Enzyme Stability
  • Galactose / analysis*
  • Galactose / chemistry*
  • Glucose / analysis*
  • Glucose / chemistry*
  • Kinetics
  • Materials Testing
  • Microscopy, Fluorescence
  • Microscopy, Fluorescence, Multiphoton / methods*
  • Nanomedicine / methods
  • Nanostructures / chemistry*
  • Nanostructures / ultrastructure
  • Particle Size
  • Protein Binding

Substances

  • Capsules
  • Glucose
  • Galactose