Discovery of 2-[5-(4-chloro-phenyl)-1-(2,4-dichloro-phenyl)-4-ethyl-1H-pyrazol-3-yl]-1,5,5-trimethyl-1,5-dihydro-imidazol-4-thione (BPR-890) via an active metabolite. A novel, potent and selective cannabinoid-1 receptor inverse agonist with high antiobesity efficacy in DIO mice

J Med Chem. 2009 Jul 23;52(14):4496-510. doi: 10.1021/jm900471u.

Abstract

By using the active metabolite 5 as an initial template, further structural modifications led to the identification of the titled compound 24 (BPR-890) as a highly potent CB1 inverse agonist possessing an excellent CB2/1 selectivity and remarkable in vivo efficacy in diet-induced obese mice with a minimum effective dose as low as 0.03 mg/kg (po qd) at the end of the 30-day chronic study. Current SAR studies along with those of many existing rimonabant-mimicking molecules imply that around the pyrazole C3-position, a rigid and deep binding pocket should exist for CB1 receptor. In addition, relative to the conventional carboxamide carbonyl, serving as a key hydrogen-bond acceptor during ligand-CB1 receptor interaction, the corresponding polarizable thione carbonyl might play a more critical role in stabilizing the Asp366-Lys192 salt bridge in the proposed CB1-receptor homology model and inducing significant selectivity for CB1R over CB2R.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Anti-Obesity Agents / chemistry
  • Anti-Obesity Agents / metabolism
  • Anti-Obesity Agents / pharmacology
  • Anti-Obesity Agents / therapeutic use
  • Cell Line
  • Diabetes Mellitus / chemically induced
  • Diabetes Mellitus / drug therapy*
  • Diabetes Mellitus / metabolism
  • Diet
  • Drug Discovery*
  • Drug Inverse Agonism*
  • Eating / drug effects
  • Humans
  • Imidazoles / chemistry
  • Imidazoles / metabolism*
  • Imidazoles / pharmacology*
  • Imidazoles / therapeutic use
  • Inhibitory Concentration 50
  • Male
  • Mice
  • Mice, Obese
  • Rats
  • Receptor, Cannabinoid, CB1 / agonists*
  • Receptor, Cannabinoid, CB2 / agonists
  • Substrate Specificity
  • Thiones / chemistry
  • Thiones / metabolism*
  • Thiones / pharmacology*
  • Thiones / therapeutic use

Substances

  • 2-(5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-ethyl-1H-pyrazol-3-yl)-1,5,5-trimethyl-1,5-dihydroimidazol-4-thione
  • Anti-Obesity Agents
  • Imidazoles
  • Receptor, Cannabinoid, CB1
  • Receptor, Cannabinoid, CB2
  • Thiones
  • imidazole