Stabilization of imidosamarium(III) cubane by amidinates

Inorg Chem. 2009 Jul 20;48(14):6344-6. doi: 10.1021/ic900808f.

Abstract

An imidosamarium(III) cubane has been prepared from the reductive cleavage of azobenzene by a divalent samarium bis(amidinate) complex, indicating that the "spectrator" bis(amidinate) and the resulting imido ligands help to stabilize the cubane framework. The cubane-type imido cluster is a novel unit in lanthanide chemistry.