Excised damaged base determines the turnover of human N-methylpurine-DNA glycosylase

DNA Repair (Amst). 2009 Oct 2;8(10):1201-6. doi: 10.1016/j.dnarep.2009.06.005. Epub 2009 Jul 17.

Abstract

N-Methylpurine-DNA glycosylase (MPG) initiates base excision repair in DNA by removing a wide variety of alkylated, deaminated, and lipid peroxidation-induced purine adducts. In this study, we tested the role of excised base on MPG enzymatic activity. After the reaction, MPG produced two products: free damaged base and AP-site containing DNA. Our results showed that MPG excises 1,N(6)-ethenoadenine (varepsilonA) from varepsilonA-containing oligonucleotide (varepsilonA-DNA) at a similar or slightly increased efficiency than it does hypoxanthine (Hx) from Hx-containing oligonucleotide (Hx-DNA) under similar conditions. Real-time binding experiments by surface plasmon resonance (SPR) spectroscopy suggested that both the substrate DNAs have a similar equilibrium binding constant (K(D)) towards MPG, but under single-turnover (STO) condition there is apparently no effect on catalytic chemistry; however, the turnover of the enzyme under multiple-turnover (MTO) condition is higher for varepsilonA-DNA than it is for Hx-DNA. Real-time binding experiments by SPR spectroscopy further showed that the dissociation of MPG from its product, AP-site containing DNA, is faster than the overall turnover of either Hx- or varepsilonA-DNA reaction. We thereby conclude that the excised base plays a critical role in product inhibition and, hence, is essential for MPG glycosylase activity. Thus, the results provide the first evidence that the excised base rather than AP-site could be rate-limiting for DNA-glycosylase reactions.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Adenine / analogs & derivatives
  • Adenine / metabolism
  • Base Sequence
  • Binding Sites
  • DNA / chemistry
  • DNA / genetics*
  • DNA / metabolism*
  • DNA Damage*
  • DNA Glycosylases / chemistry
  • DNA Glycosylases / metabolism*
  • Enzyme Stability
  • Glycosides / chemistry
  • Humans
  • Hypoxanthine / metabolism
  • Kinetics
  • Molecular Sequence Data
  • Surface Plasmon Resonance

Substances

  • Glycosides
  • 1,N(6)-ethenoadenine
  • Hypoxanthine
  • DNA
  • DNA Glycosylases
  • DNA-3-methyladenine glycosidase II
  • Adenine