Synthesis of gold nanorod-embedded polymeric nanoparticles by a nanoprecipitation method for use as photothermal agents

Nanotechnology. 2009 Sep 9;20(36):365602. doi: 10.1088/0957-4484/20/36/365602. Epub 2009 Aug 18.

Abstract

For the synthesis of biocompatible photothermal agents, gold nanorod-embedded polymeric nanoparticles (GPNs) were synthesized using a nanoprecipitation method. Uniform gold nanorods (GNRs), which are sensitive to a photothermal effect by near-infrared (NIR) light, with an aspect ratio of 4.0 were synthesized by a seed-mediated growth method. The hydroxyl groups of polycaprolactone diol (PCL diOH) were modified by esterification with mercaptopropionic acid to give a dithiol (polycaprolactone dithiol, PCL diSH) as a phase transfer and capping agent. Subsequently, hexadecyltrimethylammonium bromide (CTAB), a stabilizer of GNRs, was exchanged and/or removed by PCL diSH. PCL diSH-coated GNRs were further wrapped in a hydrophilic polymer, Pluronic F127, as a stabilizer. These newly formulated GPNs exhibit excellent stability in water and a maximum absorbance in the NIR region indicating a highly efficient surface plasmon resonance effect, phenomena useful for photothermal agents.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biocompatible Materials / chemistry
  • Chemical Precipitation
  • Gold / chemistry*
  • Metal Nanoparticles / chemistry*
  • Microscopy, Electron, Transmission
  • Nanotechnology / methods*
  • Photochemical Processes
  • Polyesters / chemistry*
  • Spectroscopy, Fourier Transform Infrared
  • Spectroscopy, Near-Infrared
  • Temperature

Substances

  • Biocompatible Materials
  • Polyesters
  • polycaprolactone
  • Gold