A novel S3S-TAP-tag for the isolation of T-cell interaction partners of adhesion and degranulation promoting adaptor protein

Proteomics. 2009 Dec;9(23):5288-95. doi: 10.1002/pmic.200900294.

Abstract

The identification of modular units of cellular function is a major goal for proteomic research. Protein complexes represent important building blocks defining functionality and deciphering their composition remains a major challenge. Here, we have designed a new tandem affinity purification (TAP) tag (termed S3S-tag) for the isolation of protein complexes. Specifically, the immune cell protein ADAP that regulates integrin adhesion was fused either C- or N-terminally to the S3S-tag. After retroviral transduction of a vector containing S3S-tagged ADAP and internal ribosomal entry site encoded enhanced green fluorescent protein (eGFP), Jurkat T cells were sorted according to eGFP expression and further selected for expression of TAP-tagged protein close to endogenous levels. The combination of a cleavable S-tag and a Strep-tag II allowed for the isolation of ADAP and associated proteins. Subsequently, stable isotope labeling with amino acids in cell culture-based mass spectrometric analysis was performed to identify potentially specific interaction partners. Co-purification of the known interaction partner Src kinase-associated phosphoprotein of 55 kDa indicates the validity of our approach, while the identification of the ENA/VASP family member EVL, the guanine nucleotide exchange factor GEF-H1 and the adaptor protein DOCK2 corroborates a link between ADAP-mediated integrin regulation and the cytoskeleton.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adaptor Proteins, Signal Transducing / analysis*
  • Adaptor Proteins, Signal Transducing / genetics
  • Adaptor Proteins, Signal Transducing / metabolism*
  • Amino Acid Sequence
  • Base Sequence
  • Cell Adhesion Molecules / analysis
  • Cell Adhesion Molecules / metabolism
  • Electrophoresis, Gel, Two-Dimensional
  • Flow Cytometry
  • GTPase-Activating Proteins
  • Gene Expression
  • Genetic Vectors / genetics
  • Guanine Nucleotide Exchange Factors / analysis
  • Guanine Nucleotide Exchange Factors / metabolism
  • Humans
  • Jurkat Cells
  • Lymphocyte Activation
  • Mass Spectrometry
  • Molecular Sequence Data
  • Phosphoproteins / analysis
  • Phosphoproteins / metabolism
  • Protein Interaction Mapping / methods*
  • Rho Guanine Nucleotide Exchange Factors
  • T-Lymphocytes / immunology
  • T-Lymphocytes / metabolism*
  • Transfection

Substances

  • ARHGEF2 protein, human
  • Adaptor Proteins, Signal Transducing
  • Cell Adhesion Molecules
  • DOCK2 protein, human
  • EVL protein, human
  • FYB1 protein, human
  • GTPase-Activating Proteins
  • Guanine Nucleotide Exchange Factors
  • Phosphoproteins
  • Rho Guanine Nucleotide Exchange Factors
  • SKAP1 protein, human