Identifying modulators of protein-protein interactions using photonic crystal biosensors

J Am Chem Soc. 2009 Dec 30;131(51):18202-3. doi: 10.1021/ja907066r.

Abstract

Inhibitors and activators of protein-protein interactions are valuable as biological probes and medicinal agents but are often difficult to identify. Herein we describe a high-throughput assay, based upon photonic crystal (PC) biosensors, for the identification of modulators of protein-protein interactions. Through the use of a d-biotin-tris-NTA (BTN) hybrid compound, any His6-tagged protein can be immobilized on the surface of a PC biosensor. Binding of the bound protein to its cognate partner is detected via a shift in the peak wavelength value. We demonstrate this assay with three protein-protein pairs (caspase-9-XIAP, caspase-7-XIAP, FKBP12-FRB) and their small molecule modulators.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biosensing Techniques / methods*
  • Drug Discovery / methods*
  • Humans
  • Immobilized Proteins
  • Optics and Photonics / methods
  • Protein Binding / drug effects*
  • Proteins / chemistry*
  • Proteins / metabolism

Substances

  • Immobilized Proteins
  • Proteins