From silphinenes to penifulvins: a biomimetic approach to penifulvins B and C

Org Lett. 2010 Jan 15;12(2):272-5. doi: 10.1021/ol902594b.

Abstract

The biomimetic total synthesis of penifulvins B and C uses a meta-photocycloaddition as a key step which gives rapid access to the fenestrane-type carboskeleton with control of an onring quaternary stereocenter. The route is concise, stereocontrolled, scaleable, and flexibile and requires only one protecting group.

MeSH terms

  • Biomimetics*
  • Cyclization
  • Molecular Conformation
  • Sesquiterpenes / chemical synthesis*
  • Sesquiterpenes / chemistry
  • Stereoisomerism

Substances

  • Sesquiterpenes
  • penifulvin B
  • penifulvin C