[Pressurized liquid extraction of Tripterygiumw wilfordii polyglycosides and optimization of extraction conditions]

Zhongguo Zhong Yao Za Zhi. 2010 Jan;35(1):44-8. doi: 10.4268/cjcmm20100109.
[Article in Chinese]

Abstract

Objective: To investigate the extraction method of polyglycosides from Tripterygium wilfordii.

Method: The extraction method of pressurized liquid extraction was employed and chromogenic colorimetric technique were used for quantitative analysis. Based on the single-factor experiment, according to the center combination design this paper used three factors and three levels of response surface methodology for process optimization.

Result: The optimized conditions were as follows: ratio of solid to liquid was 1:9.5, at the temperature of 115 degrees C for 80 minutes, the actual extract ratio and purity of polyglycosides obtained were 0.21% and 0.52%, respectively.

Conclusion: The method of pressurized liquid extraction has obvious advantages over conventional reflux extracting.

Publication types

  • English Abstract

MeSH terms

  • Glycosides / isolation & purification*
  • Plant Extracts / chemistry*
  • Pressure
  • Tripterygium / chemistry*

Substances

  • Glycosides
  • Plant Extracts