Exploring the "forgotten"-OH NMR spectral region in natural products

Chem Commun (Camb). 2010 May 28;46(20):3589-91. doi: 10.1039/b927256a. Epub 2010 Apr 7.

Abstract

Significantly enhanced resolution in the -OH NMR spectral region was observed which, in combination with 2D (1)H-(13)C HMBC techniques, will open new avenues in structure analysis of natural products with phenol type -OH groups in complex natural extracts without the need of laborious isolation of the individual compounds.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biological Factors / chemistry*
  • Carbon Isotopes
  • Dimethyl Sulfoxide / chemistry
  • Hydrogen-Ion Concentration
  • Hydroxyl Radical / chemistry*
  • Magnetic Resonance Spectroscopy
  • Molecular Structure
  • Protons
  • Solutions
  • Stereoisomerism

Substances

  • Biological Factors
  • Carbon Isotopes
  • Protons
  • Solutions
  • Hydroxyl Radical
  • Dimethyl Sulfoxide