Base-promoted one-pot tandem reaction of 3-(1-alkynyl)chromones under microwave irradiation to functionalized amino-substituted xanthones

J Org Chem. 2010 Sep 17;75(18):6304-7. doi: 10.1021/jo1013614.

Abstract

A base-promoted one-pot tandem reaction has been developed from 3-(1-alkynyl)chromones with various acetonitriles to afford functionalized amino-substituted xanthones 3 under microwave irradiation. This tandem process involves multiple reactions, such as Michael addition/cyclization/1,2-addition, without a transition metal catalyst. This method provides an efficient approach to build up natural product-like diversified amino-substituted xanthone scaffolds rapidly.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Chromones / chemical synthesis*
  • Chromones / chemistry
  • Microwaves*
  • Molecular Structure
  • Stereoisomerism
  • Xanthones / chemistry*

Substances

  • Chromones
  • Xanthones