Synthesis and in vitro antiviral activities of 3'-fluoro (or chloro) and 2',3'-difluoro 2',3'-dideoxynucleoside analogs against hepatitis B and C viruses

Bioorg Med Chem. 2010 Nov 1;18(21):7542-7. doi: 10.1016/j.bmc.2010.08.048. Epub 2010 Sep 23.

Abstract

Chronic infections with hepatitis B virus (HBV) and hepatitis C virus (HCV) lead to serious liver diseases worldwide. Co-infection with HBV and HCV is very common and is associated with increased risk of liver pathogenesis, liver cancer, and liver failure. Several 5-substituted 3'-fluoro (or chloro) (1-4, 6, 7, 17-19) and 2',3'-difluoro 2',3'-dideoxynucleosides (15 and 16) were synthesized and evaluated for in vitro antiviral activities against duck hepatitis B virus (DHBV), human hepatitis B virus, and hepatitis C virus. Of these compounds 4, 7, 17, and 19 demonstrated moderate anti-HBV activity, and 2, 4, 7, 8, and 19 were weak inhibitors of HCV. Although 5-iodo derivative (7) was most inhibitory against HCV, it exhibited a reduction in cellular RNA levels in Huh-7 cells. The 5-hydroxymethyl-3'-fluoro-2',3'-dideoxyuridine (4) and 1-(3-chloro-2,3-dideoxy-β-d-erythro-pentofuranosyl)-5-fluorouracil (19) provided the most inhibition of both viruses without cytotoxicity.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Antiviral Agents / chemical synthesis*
  • Antiviral Agents / chemistry
  • Antiviral Agents / pharmacology
  • Cell Line, Tumor
  • DNA, Viral / metabolism
  • Dideoxynucleosides / chemical synthesis
  • Dideoxynucleosides / chemistry*
  • Dideoxynucleosides / pharmacology
  • Hepacivirus / drug effects*
  • Hepatitis B Virus, Duck / drug effects
  • Hepatitis B virus / drug effects*
  • Humans
  • RNA, Viral / metabolism

Substances

  • Antiviral Agents
  • DNA, Viral
  • Dideoxynucleosides
  • RNA, Viral
  • 3'-fluoro-2',3'-dideoxyuridine
  • 2',3'-dideoxyuridine